Amazing Spider-Man 1963 - vol. 1 #1 by Stan Lee, Steve Ditko

By Stan Lee, Steve Ditko

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Despite these limitations, it is concluded that TPS with mass spectrometric detection is a highly useful technique for studying the sulfidation of hydrotreating catalysts. We return to the sulfidation of molybdenum oxides in Chapter 3 (photoemission), Chapter 4 (ion spectroscopy), and also in a case study on hydrodesulfurization catalysts (Chapter 9). 4 Temperature-Programmed Reaction Spectroscopy Important information on reaction mechanisms and on the influence of promoters can be deduced from temperature-programmed reactions [2].

We refer to Margaritondo [4] for an interesting review on the early days of the photoelectric effect. It was a half-century later before the photoelectric effect was applied in spectroscopy. As described by Ertl and Ku¨ppers [5], three parallel developments took place:  During the 1950s, Siegbahn’s group worked to improve the energy resolution of electron spectrometers and then to combine it with X-ray sources. This led to a technique called electron spectroscopy for chemical analysis (ESCA), which today is more commonly referred to as X-ray photoelectron spectroscopy (XPS) 40 3 Photoemission and Auger Spectroscopy [6].

9 Examples of temperatureprogrammed desorption following zeroth-, first- and second-order kinetics. Each curve corresponds to a different initial coverage of the adsorbate. Ag/Ru(001): Silver forms islands on the ruthenium substrate. Desorption of Ag from the edges of these islands gives rise to zeroth-order kinetics; note the exponential increase of the lowtemperature sides of the peak, as expected from Eq. (2-15). Desorption from the second layer of silver occurs at lower temperatures, indicating that AgaAg bonds are weaker than AgaRu bonds [20].

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